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Preparation of Stable Microemulsions with Different Droplet Size

Received: 7 November 2019     Accepted: 28 November 2019     Published: 10 December 2019
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Abstract

Microemulsion is a widely used technique for preparing nanoparticles. The droplet size in stable microemulsions is a key parameter for limiting the size and shape of the formed nanoparticles. In this paper, the stable microemulsions were synthesized by two titration methods, the water titration method and the co-surfactant titration. Six reagents with different HLB were used as surfactants, including Span-80, E-1302, EL-10, MOA-9, Triton X-114 and OP-10. Quasi ternary phase diagrams of O/W and W/O microemusions with different surfactants were established according to the composition of surfactant, co-surfactant, oil and water. The size of the microemulsions droplets was characterized by using Zetasizer Nano S90. Within the stable micromulsions region, the droplet size was systemically controlled from 1 nm to 120 nm by changing different surfactants and controlling the quality ratio of components. A complex dependence of the droplet size on the water to surfactant ratio and the co-surfactant to surfactant ratio was established. In the stable microemulsions region, the droplets size increases dramatically with increased the water to surfactant ratio and the larger droplet size is obtained with increasing the co-surfactant amount.

Published in American Journal of Nanosciences (Volume 5, Issue 4)
DOI 10.11648/j.ajn.20190504.18
Page(s) 76-82
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2019. Published by Science Publishing Group

Keywords

Microemulsions, Quasi Ternary Phase, Droplet Size

References
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Cite This Article
  • APA Style

    Hu Shiyu, Chen Jiaxuan, Zhu Yeting, Wei Yelu, Di Tongtong, et al. (2019). Preparation of Stable Microemulsions with Different Droplet Size. American Journal of Nanosciences, 5(4), 76-82. https://doi.org/10.11648/j.ajn.20190504.18

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    ACS Style

    Hu Shiyu; Chen Jiaxuan; Zhu Yeting; Wei Yelu; Di Tongtong, et al. Preparation of Stable Microemulsions with Different Droplet Size. Am. J. Nanosci. 2019, 5(4), 76-82. doi: 10.11648/j.ajn.20190504.18

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    AMA Style

    Hu Shiyu, Chen Jiaxuan, Zhu Yeting, Wei Yelu, Di Tongtong, et al. Preparation of Stable Microemulsions with Different Droplet Size. Am J Nanosci. 2019;5(4):76-82. doi: 10.11648/j.ajn.20190504.18

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  • @article{10.11648/j.ajn.20190504.18,
      author = {Hu Shiyu and Chen Jiaxuan and Zhu Yeting and Wei Yelu and Di Tongtong and Shen Hangyan},
      title = {Preparation of Stable Microemulsions with Different Droplet Size},
      journal = {American Journal of Nanosciences},
      volume = {5},
      number = {4},
      pages = {76-82},
      doi = {10.11648/j.ajn.20190504.18},
      url = {https://doi.org/10.11648/j.ajn.20190504.18},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajn.20190504.18},
      abstract = {Microemulsion is a widely used technique for preparing nanoparticles. The droplet size in stable microemulsions is a key parameter for limiting the size and shape of the formed nanoparticles. In this paper, the stable microemulsions were synthesized by two titration methods, the water titration method and the co-surfactant titration. Six reagents with different HLB were used as surfactants, including Span-80, E-1302, EL-10, MOA-9, Triton X-114 and OP-10. Quasi ternary phase diagrams of O/W and W/O microemusions with different surfactants were established according to the composition of surfactant, co-surfactant, oil and water. The size of the microemulsions droplets was characterized by using Zetasizer Nano S90. Within the stable micromulsions region, the droplet size was systemically controlled from 1 nm to 120 nm by changing different surfactants and controlling the quality ratio of components. A complex dependence of the droplet size on the water to surfactant ratio and the co-surfactant to surfactant ratio was established. In the stable microemulsions region, the droplets size increases dramatically with increased the water to surfactant ratio and the larger droplet size is obtained with increasing the co-surfactant amount.},
     year = {2019}
    }
    

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  • TY  - JOUR
    T1  - Preparation of Stable Microemulsions with Different Droplet Size
    AU  - Hu Shiyu
    AU  - Chen Jiaxuan
    AU  - Zhu Yeting
    AU  - Wei Yelu
    AU  - Di Tongtong
    AU  - Shen Hangyan
    Y1  - 2019/12/10
    PY  - 2019
    N1  - https://doi.org/10.11648/j.ajn.20190504.18
    DO  - 10.11648/j.ajn.20190504.18
    T2  - American Journal of Nanosciences
    JF  - American Journal of Nanosciences
    JO  - American Journal of Nanosciences
    SP  - 76
    EP  - 82
    PB  - Science Publishing Group
    SN  - 2575-4858
    UR  - https://doi.org/10.11648/j.ajn.20190504.18
    AB  - Microemulsion is a widely used technique for preparing nanoparticles. The droplet size in stable microemulsions is a key parameter for limiting the size and shape of the formed nanoparticles. In this paper, the stable microemulsions were synthesized by two titration methods, the water titration method and the co-surfactant titration. Six reagents with different HLB were used as surfactants, including Span-80, E-1302, EL-10, MOA-9, Triton X-114 and OP-10. Quasi ternary phase diagrams of O/W and W/O microemusions with different surfactants were established according to the composition of surfactant, co-surfactant, oil and water. The size of the microemulsions droplets was characterized by using Zetasizer Nano S90. Within the stable micromulsions region, the droplet size was systemically controlled from 1 nm to 120 nm by changing different surfactants and controlling the quality ratio of components. A complex dependence of the droplet size on the water to surfactant ratio and the co-surfactant to surfactant ratio was established. In the stable microemulsions region, the droplets size increases dramatically with increased the water to surfactant ratio and the larger droplet size is obtained with increasing the co-surfactant amount.
    VL  - 5
    IS  - 4
    ER  - 

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Author Information
  • College of Materials and Chemistry, China Jiliang University, Hangzhou, China

  • College of Materials and Chemistry, China Jiliang University, Hangzhou, China

  • College of Materials and Chemistry, China Jiliang University, Hangzhou, China

  • College of Materials and Chemistry, China Jiliang University, Hangzhou, China

  • College of Materials and Chemistry, China Jiliang University, Hangzhou, China

  • College of Materials and Chemistry, China Jiliang University, Hangzhou, China

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